Effects of Different Pretreatments Combined with Steam Explosion on the Properties of Bamboo Fibers

Authors

  • Yanping Zou Nanjing Forestry University, Zhejiang Academy of Forestry, Key Laboratory of Bamboo Research of Zhejiang Province
  • Wenfu Zhang Zhejiang Academy of Forestry, Key Laboratory of Bamboo Research of Zhejiang Province
  • Shaofei Yuan Zhejiang Academy of Forestry, Key Laboratory of Bamboo Research of Zhejiang Province
  • Jian Zhang Zhejiang Academy of Forestry, Key Laboratory of Bamboo Research of Zhejiang Province
  • Hong Chen Nanjing Forestry University

Keywords:

Bamboo fibers (BFs), Pretreatment, Steam explosion (SE), Microstructure, X-ray photoelectron spectroscopy (XPS)

Abstract

Bamboo pretreatment is a key technology for the preparation of bamboo fibers (BFs) for composites. This study examined the properties of BFs prepared by steam explosion (SE) BFs following pretreatment by enzyme, alkali, and salt. The microstructure, functional groups, crystallinity, and surface chemical elements of BFs were characterized by environmental scanning electron microscope (ESEM), Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), and X-ray photoelectron spectroscopy (XPS). The results indicated that bamboo could be separated into fiber bundles through SE after pretreatment. The separation of BFs pretreated by enzyme and alkali were better, but colloid remained and was able to stick the fibers together. Through performing different pretreatments before SE, the lignin and hemicellulose of BFs were partially removed, and alkali pretreatment had the best effect on lignin removal. The crystal structure of the BFs did not change significantly, and the crystallinity of BFs was highest at 2 MPa and 6 min when pretreated by alkali. The XPS results showed that the effect of alkali pretreatment at 2 MPa for 6 min was the best.

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Published

2022-12-05

Issue

Section

Research Article or Brief Communication